High resolution partition capillary columns
β Scribed by A. Liberti; L. Zoccolillo
- Publisher
- Elsevier Science
- Year
- 1970
- Tongue
- English
- Weight
- 268 KB
- Volume
- 49
- Category
- Article
- ISSN
- 1873-3778
No coin nor oath required. For personal study only.
β¦ Synopsis
Various procedures to obtain high resolution glass capillary columns are described. By roughening the glass surface either with a layer of carbon or with polymerised material, a stationary phase of any polarity can bb successfully coated. Results obtained with Carbowax, trimer acid and squalane columns are reported; the separation of polar and non-polar compounds from their deuterated homologs (C
π SIMILAR VOLUMES
This series is intended to present the basic theory of chromatography in simple and clear mathematics which can be readily followed by the average chemist. The basic ideas are not necessarily novel but the approach and applications should be original and of interest to a large number of workers in c
## Abstract A rapid and specific procedure is described for the resolution of nine steroids present in conjugated estrogen preparations. Resolution is achieved on a short glass capillary column coated with Silar 10C after dual derivatization to oximeβtrimethylsilyl ethers.