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Heterocyclic Studies. V. Proof of Structure and Synthesis of 3-Hydroxy-4-methyl-5-phenylpyridine, A Degradation Product of 2,3-Dihydro-5-methyl-6-phenyl-4H-1,2-diazepin-4-one 1

✍ Scribed by Moore, James A.; Püschner, Heinz H.

Book ID
126434611
Publisher
American Chemical Society
Year
1959
Tongue
English
Weight
709 KB
Volume
81
Category
Article
ISSN
0002-7863

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The title compound 3 was obtained during the rearrangement of isoxazol-5-yl hydrazine 1 to 1 -aminopyrazolone 2 at \(115^{\circ}\). X-ray analysis of the corresponding benzylidene derivative allowed us to achieve the structure assignment.