✦ LIBER ✦

Fluorometric analysis of pectenotoxin-2 in microalgal samples by high performance liquid chromatography

✍ Scribed by Katsunoti Sasaki; Azusa Takizawa; Aurelia Tubaro; Laura Sidari; Roberto Della Loggia; Takeshi Yasumoto

Publisher: John Wiley and Sons
Year: 1999
Tongue: English
Weight: 77 KB
Volume: 7
Category: Article
ISSN: 1056-9014
DOI: 10.1002/1522-7189(199911/12)7:6<241::aid-nt66>3.0.co;2-g

No coin nor oath required. For personal study only.

✦ Synopsis

A rapid HPLC method with ¯uorescence detection of pectenotoxin-2 (PTX2), a polyether macrolide toxin, in microalgae is presented. A dienophile reagent, DMEQ-TAD, was used for precolumn ¯uorescence labeling. PTX2 could be quantitatively detected in the range 1±200 ng. This method con®rmed the occurrence of PTX2 in net haul samples mostly composed of dino¯agellates Dinophysis spp. collected in the Adriatic Sea, Italy and Mutsu Bay, Japan.

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