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Flow injection, amperometric determination of ethanol in wines after solid-phase extraction

✍ Scribed by Zuliang Chen; Ji Jin Yu; D. Brynn Hibbert

Publisher
John Wiley and Sons
Year
1997
Tongue
English
Weight
302 KB
Volume
9
Category
Article
ISSN
1040-0397

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✦ Synopsis

Ethanol in wines was determined by flow injection analysis with an amperometric detector using an oxidized nickel wire. Solid-phase extraction with a strong anion exchanger was used to remove interferences such as organic acids from the matrix, and the residue of the extraction was injected directly into the FIA system. The recoveries of ethanol from wines spiked with standards ranged from 101 % to 103 %. The response of the nickel electrode to ethanol is dependent on the applied potential and the pH of the carrier. The optimal conditions for the detection of ethanol were an applied potential of +0.60 V (vs. Ag/AgC1) in a carrier of 100 mM sodium hydroxide solution. The electrode exhibited a linear response from to lo-' M, with a detection limit of 1 x

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