𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Fast liquid chromatography for the resolution of chiral compounds

✍ Scribed by Scott R. Perrin

Publisher
John Wiley and Sons
Year
1991
Tongue
English
Weight
484 KB
Volume
3
Category
Article
ISSN
0899-0042

No coin nor oath required. For personal study only.

✦ Synopsis

A Pirkle-concept chiral stationary phase (CSP) derived from N-(1-naphthy1)leucine was evaluated for developing methods to reduce analysis times and investigating techniques in the rapid screening of a variety of chiral compounds over a given chiral selector. The effects of reduced column lengths and elevated temperatures were studied to shorten analysis times.

πŸ“œ SIMILAR VOLUMES

Chiral recognition in liquid chromatogra
Chiral recognition in liquid chromatography utilising chargeable cyclodextrins for resolution of doxazosin enantiomers
✍ Paul K. Owens; Anthony F. Fell; Michael W. Coleman; John C. Berridge πŸ“‚ Article πŸ“… 1997 πŸ› John Wiley and Sons 🌐 English βš– 235 KB πŸ‘ 1 views

The chromatographic resolution of rac-doxazosin using reversed-phase high performance liquid chromatography (HPLC) with the chargeable chiral mobile phase additive, carboxymethyl-beta-cyclodextrin (CM-beta-CD), is described. The effects of different modifiers (acetonitrile, methanol and tetrahydrofu

Optical resolution of some biologically
Optical resolution of some biologically active compounds by chiral liquid chromatography on BSA-silica (resolvosil) columns
✍ Stig Allenmark; Shalini Andersson πŸ“‚ Article πŸ“… 1989 πŸ› John Wiley and Sons 🌐 English βš– 443 KB

Optical resolution on the analytical scale of a number of racemic pharmaceuticals and some other biologically active compounds has been studied using immobilized bovine serum albumin (BSA) as the stationary phase. For some of the compounds the elution order was determined by the use of optically enr

Fast Liquid Chromatography for High-Thro
Fast Liquid Chromatography for High-Throughput Screening of Polymers
✍ Harald Pasch; Peter Kilz πŸ“‚ Article πŸ“… 2003 πŸ› John Wiley and Sons 🌐 English βš– 103 KB πŸ‘ 1 views

## Abstract Liquid chromatography of polymers is traditionally a slow technique with analysis times of typically 30 min per sample. For the application of liquid chromatographic techniques to combinatorial materials research the analysis time per sample must be reduced considerably. Analysis time i

Enantiomeric resolution of new triazole
Enantiomeric resolution of new triazole compounds by high-performance liquid chromatography
✍ Chunguang Lv; Guifang Jia; Wentao Zhu; Jing Qiu; Xinquan Wang; Zhiqiang Zhou πŸ“‚ Article πŸ“… 2007 πŸ› John Wiley and Sons 🌐 English βš– 452 KB

## Abstract Cellulose tris(3,5‐dimethylphenylcarbamate) (CDMPC) was synthesized and coated on aminopropylsilica to prepare a chiral stationary phase (CSP). HPLC methods were developed for the direct enantioseparation of 12 chiral triazole compounds on the CSP. The separations were made using normal

Chiral resolution of flobufen by high pe
Chiral resolution of flobufen by high performance liquid chromatography and capillary electrophoresis
✍ Eva TesarvΓ‘; Martin Gila; Alexandr Jegorov; M. UhrovΓ‘; Zdenck Deyl πŸ“‚ Article πŸ“… 1997 πŸ› John Wiley and Sons 🌐 English βš– 119 KB πŸ‘ 2 views

The enantiomeric separation of an anti-inflammatory drug flobufen was performed on various chiral columns in liquid chromatography and by reversed phase chromatography and by capillary electrophoresis with ␀cyclodextrin as a chiral selector in the mobile phase and background electrolyte, respectivel