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Facile Epoxidation of α,β-Unsaturated Ketones with Cyclohexylidenebishydroperoxide.

✍ Scribed by Kavitha Jakka; Jinyun Liu; Cong-Gui Zhao

Publisher
John Wiley and Sons
Year
2007
Weight
28 KB
Volume
38
Category
Article
ISSN
0931-7597

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Dioxirane Epoxidation of α,β-Unsaturated
Dioxirane Epoxidation of α,β-Unsaturated Ketones
✍ Adam, Waldemar ;Hadjiarapoglou, Lazaros ;Smerz, Alex 📂 Article 📅 1991 🏛 Wiley (John Wiley & Sons) 🌐 English ⚖ 717 KB

## 2-Cycloen-1 -ones / Caroate The synthesis of epoxides 3ar is achieved in excellent yields by reaction of the a,P-unsaturated ketones l a -c , 4,4'-disubstituted (E)-chalcones 1 d -0 , and 2'-hydroxy-4-substituted (E)chalcones l p -r with isolated dimethyldioxirane (2a) (as ac-etone solution) an