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fac-Tri­aqua­[tris(2-pyridyl)­amine-κ3N]­chromium(III) tris­(tri­fluoro­methane­sulfonate)

✍ Scribed by Terasaki, Yukiko ;Fujihara, Takashi ;Nagasawa, Akira ;Kaizaki, Sumio

Publisher
International Union of Crystallography
Year
2004
Tongue
English
Weight
241 KB
Volume
60
Category
Article
ISSN
1600-5368

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✍ Li, Xiaoju ;Cao, Rong ;Sun, Daofeng ;Bi, Wenhua ;Wang, Yanqin ;Hong, Maochun 📂 Article 📅 2003 🏛 International Union of Crystallography 🌐 English ⚖ 204 KB

The title compound, {[Ag(bpe)](OTf)} n (OTf = tri¯uoromethanesulfonate) or {[Ag(C 12 H 12 N 2 )](CF 3 O 3 S)} n , has been prepared from the reaction of 1,2-bis(4-pyridyl)ethane (bpe) and Ag(CF 3 SO 3 ) in MeCN/H 2 O. The Ag I atom is twocoordinate in a slightly distorted linear arrangement, and the

(2,2′-Bipyridyl-N,N′)(bi­cyclo­[3.3.1]­n
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✍ Ma, Kuangbiao ;Bats, Jan W. ;Wagner, Matthias 📂 Article 📅 2001 🏛 International Union of Crystallography 🌐 English ⚖ 308 KB

The cations and anions in the title compound, C 18 H 22 BN 2 + ÁCF 3 SO 3 ## À , are connected by intermolecular CÐ HÁ Á ÁO hydrogen bonds, with HÁ Á ÁO distances between 2.34 and 2.60 A Ê , into layers parallel to the bc plane.