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(2,2′-Bipyridyl-N,N′)(bi­cyclo­[3.3.1]­nonane-C1,C5)­boronium tri­fluoro­methane­sulfonate

✍ Scribed by Ma, Kuangbiao ;Bats, Jan W. ;Wagner, Matthias

Publisher
International Union of Crystallography
Year
2001
Tongue
English
Weight
308 KB
Volume
57
Category
Article
ISSN
1600-5368

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✦ Synopsis

The cations and anions in the title compound, C 18 H 22 BN 2 + ÁCF 3 SO 3

À

, are connected by intermolecular CÐ HÁ Á ÁO hydrogen bonds, with HÁ Á ÁO distances between 2.34 and 2.60 A Ê , into layers parallel to the bc plane.

📜 SIMILAR VOLUMES

cis-(2,2′-Bipyridyl-κ2N,N′)­carbonyl(η3-
cis-(2,2′-Bipyridyl-κ2N,N′)­carbonyl(η3-1-methyl­ene-2,2′:6′,2′′-terpyridyl-κ3C1,N,N′)ruthenium(II) bis­(hexa­fluoro­phosphate) acetone disolvate
✍ Gibson, Dorothy H. ;Mashuta, Mark S. ;Andino, Jose G. 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 217 KB

Single-crystal X-ray study T = 90 K Mean '(C±C) = 0.005 A Ê Disorder in solvent or counterion R factor = 0.034 wR factor = 0.089 Data-to-parameter ratio = 11.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

[1,9-Bis(3,5-di­methyl­pyrazol-1-yl-κN2)
[1,9-Bis(3,5-di­methyl­pyrazol-1-yl-κN2)-3,7-di­thia­nonane-κ2S,S′]­palladium(II) bis­(tetra­fluoro­borate)
✍ García-Antón, Jordi ;Pons, Josefina ;Ros, Josep ;Solans, Xavier ;Font-Bardia, Me 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 245 KB

Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.008 A Ê Disorder in solvent or counterion R factor = 0.035 wR factor = 0.060 Data-to-parameter ratio = 18.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.