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Exchange reactions of tetrathiophosphates with thiophosphoryl chloride

✍ Scribed by P. S. Khokhlov; G. D. Sokolova; V. N. Osipov; N. F. Savenkov

Publisher
Springer
Year
1998
Tongue
English
Weight
215 KB
Volume
47
Category
Article
ISSN
1573-9171

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✍ P. J. Christen; L. M. van der Linde; F. N. Hooge πŸ“‚ Article πŸ“… 2010 πŸ› Elsevier Science 🌐 English βš– 571 KB

## Abstract The reaction of PSCl~3~, with alkylmagnesium halides has been studied. In the case of methyl‐, ethyl‐, propyl‐, butyl‐ and __iso__butyl‐magnesium halides compounds with formula (R~2~PS)~2~, were formed. Their infrared spectra were recorded from 400 cm^βˆ’1^ to 3000 cm^βˆ’1^. From these spec