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Evaluation of the efficiency of an assay procedure for gangliosides in human serum

✍ Scribed by Elena Negroni; Vanna Chigorno; Guido Tettamanti; Sandro Sonnino

Publisher: Springer US
Year: 1996
Tongue: English
Weight: 611 KB
Volume: 13
Category: Article
ISSN: 1573-4986
DOI: 10.1007/bf00731466

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Prior to GC-MS analysis, samples (1 mL) were passed through a C-18 SPE cartridge (Supelco) preconditioned with ethyl acetate, 96% (v/v) ethanol and 10% (v/v) ethanol in sequence. Resveratrol was eluted with ethyl acetate and 1 mL was collected of which 1 I~L was injected. For samples with very low c