The title compound, C~13~H~12~N~2~OS, was prepared by the reaction of (4-pyridyl)methanol with phenyl isothiocyanate and NaOH in a 1,4-dioxane solution. The asymmetric unit contains two independent molecules. The molecular structure and packing are stabilized by N—H...N intermolecular hydrogen-bond
Ethyl N-(2-pyridyl)carbamate
✍ Scribed by Zheng, Peng-Wu ;Wang, Wei ;Duan, Xue-Min
- Publisher
- International Union of Crystallography
- Year
- 2005
- Tongue
- English
- Weight
- 124 KB
- Volume
- 61
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
The title compound, C 8 H 10 N 2 O 2 , is nearly planar. The crystal packing is stabilized by N-HÁ Á ÁN hydrogen bonds.
📜 SIMILAR VOLUMES
The asymmetric unit of the title compound, C~12~H~13~N~3~O~2~·H~2~O, comprises two crystallographically independent organic molecules and two water molecules. There is an O—H...N hydrogen bond between each water molecule and the 2-substituted pyridyl ring of an organic molecule. The water molecules
The crystal structure of the title compound, C 17 H 15 BrN 2 O 2 , has been determined at room temperature. The indole moiety is essentially planar and the structure is stabilized by intra-and intermolecular NÐHÁ Á ÁO hydrogen bonds.
The title compound, C 16 H 18 N 4 S 2 , has a crystallographic inversion centre at the mid-point of the central C-C bond. The plane of the dithiooxamide fragment is approximately perpendicular to the plane of the dimethylene bridge [dihedral angle = 84.8 (1) ], the plane of which is in turn normal t
Single-crystal X-ray study T = 180 K Mean '(C±C) = 0.002 A Ê R factor = 0.034 wR factor = 0.089 Data-to-parameter ratio = 11.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.