A novel ethyl 5-cyano-6-hydroxy-2-methyl-4-(1-naphthyl)-nicotinate is successfully synthesized and the structure is determined by XRD, GC-MS analysis, element analysis and NMR spectroscopic in detail. A reaction mechanism for the reaction is proposed.
Ethyl 2-(cyclopentyloxy)-5-ethyl-4-hydroxy-6-methylnicotinate
✍ Scribed by Boland, Sandro ;Cauvin, Christine ;Norberg, Bernadette ;Le Van, Kiet ;Georges, Benoît ;Hevesi, Laszlo ;Durant, François
- Publisher
- International Union of Crystallography
- Year
- 2002
- Tongue
- English
- Weight
- 197 KB
- Volume
- 58
- Category
- Article
- ISSN
- 1600-5368
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📜 SIMILAR VOLUMES
In the title compound, C~16~H~14~N~4~O~5~, the benzene ring of the nicotinate residue is inclined at an angle of 64.06 (10)° to the benzene ring of the nitrophenoxy group. The molecules are linked by two intermolecular C—H...O and N—H...N hydrogen bonds into a complex three-dimensional framework str
In the title compound, C 12 H 16 N 4 O 3 , all bond lengths and angles are within normal ranges. An O-HÁ Á ÁN and an N-HÁ Á ÁO intramolecular hydrogen bond contribute to the approximately planar molecular conformation. In the crystal structure, intermolecular N-HÁ Á ÁO and N-HÁ Á ÁN hydrogen bonds l
The title compound, C 17 H 33 NO 7 , contains two six-membered rings which adopt chair conformations. The molecular packing is governed by intermolecular OÐHÁ Á ÁO hydrogen bonding.