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(1R,5R,6S)-6-(2-Hydroxy­ethyl)-2-methyl-5-(prop-1-en-2-yl)cyclo­hex-2-enol

✍ Scribed by Juhl, Martin ;Tanner, David ;Søtofte, Inger

Publisher
International Union of Crystallography
Year
2007
Tongue
English
Weight
272 KB
Volume
63
Category
Article
ISSN
1600-5368

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(5R,6S)-6-Methyl-5-(phenylsulfonylacetyl
(5R,6S)-6-Methyl-5-(phenylsulfonylacetyl)bicyclo[2.2.1]hept-2-ene
✍ Pei, Wen ;Wang, Yongjiang ;Sun, Mengzhan ;Xiong, Xiaobo ;Yu, Changquan 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 136 KB

The title compound, C 16 H 18 O 3 S, an endo-cycloadduct isomer, was obtained from the Diels-Alder reaction of (E)-1-(phenylsulfonyl)pent-3-en-2-one with cyclopentadiene catalysed by a chiral titanium reagent. The crystal structure confirms the absolute streochemistry.