Epoxidation of the PC Double Bond of Phosphaalkene Complexes: X-Ray Crystal Structure Analysis of a Stable Oxaphosphirane Complex
✍ Scribed by Mr. Siegfried Bauer; Dr. Angela Marinetti; Dr. Louis Ricard; Prof. Dr. François Mathey
- Publisher
- John Wiley and Sons
- Year
- 1990
- Tongue
- English
- Weight
- 282 KB
- Volume
- 29
- Category
- Article
- ISSN
- 0044-8249
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## Abstract A comprehensive ^31^P solid‐state NMR study of Ru(η^1^‐Ph~2~PCH~2~CH~2~OCH~3~)~2~(η^2^‐en)Cl~2~ (en = ethylenediamine) (1), by 1D (contact time variation, inversion–recovery, SPARTAN) and 2D techniques (homonuclear __J__‐resolved, SECSY) indicated that the crystal structure of 1 should