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Synthesis and X-ray crystal structure investigations of the complexes of a proton sponge with selected inorganic acids: Crystal structure of DMAN.HI complex

✍ Scribed by W. Łasocha; A. Rafalska-Łasocha

Publisher
John Wiley and Sons
Year
2006
Tongue
English
Weight
146 KB
Volume
41
Category
Article
ISSN
0232-1300

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## Abstract A comprehensive ^31^P solid‐state NMR study of Ru(η^1^‐Ph~2~PCH~2~CH~2~OCH~3~)~2~(η^2^‐en)Cl~2~ (en = ethylenediamine) (1), by 1D (contact time variation, inversion–recovery, SPARTAN) and 2D techniques (homonuclear __J__‐resolved, SECSY) indicated that the crystal structure of 1 should