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Enzymatic Removal of Carboxyl Protecting Groups. 2. Cleavage of the Benzyl and Methyl Moieties

✍ Scribed by Barbayianni, Efrosini; Fotakopoulou, Irene; Schmidt, Marlen; Constantinou-Kokotou, Violetta; Bornscheuer, Uwe T.; Kokotos, George

Book ID: 126088577
Publisher: American Chemical Society
Year: 2005
Tongue: English
Weight: 129 KB
Volume: 70
Category: Article
ISSN: 0022-3263
DOI: 10.1021/jo051004v

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The selective cleavage of the PMB (4-methoxybenzyl) group in the presence of the NAP (2-naphthylmethyl) group was achieved using CAN with a range of mono-saccharides. The NAP group can then be removed selectively in the presence of a benzyl group using DDQ. This provides a strategy for sequential de