An earlier two-dimensional NOESY experiment with diagonal peak suppression in the 1 H N -1 H N region is extended to three dimensions by including 15 N evolution while maintaining the TROSY approach throughout. The technique suppresses all anti-TROSY resonances by appropriate pulse sequence elements
✦ LIBER ✦
Enhanced diagonal peak suppression in three-dimensional TROSY-type15N-resolved1HN1HNNOESY spectra
✍ Scribed by Meissner, Axel ;Sørensen, Ole Winneche
- Publisher
- John Wiley and Sons
- Year
- 2001
- Tongue
- English
- Weight
- 167 KB
- Volume
- 14
- Category
- Article
- ISSN
- 1043-7347
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📜 SIMILAR VOLUMES
Three-Dimensional Protein NMR TROSY-Type
✍
Axel Meissner; Ole Winneche Sørensen
📂
Article
📅
2000
🏛
Elsevier Science
🌐
English
⚖ 94 KB
Suppression of Diagonal Peaks in TROSY-T
✍
Axel Meissner; Ole Winneche Sørensen
📂
Article
📅
1999
🏛
Elsevier Science
🌐
English
⚖ 86 KB
A novel method for suppression of diagonal peaks in the amide region of NOESY NMR spectra of 15 N-labeled proteins is presented. The method is particularly useful for larger proteins at high magnetic fields where interference between dipolar and chemical shift anisotropy relaxation mechanisms result