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Electrochemical and spectroelectrochemical studies of complexes of 1,10-phenanthroline-5,6-dione

✍ Scribed by Damien M. Murphy; Kenneth McNamara; Patricia Richardson; Veronica Sanchez-Romaguera; Richard E.P. Winpenny; Lesley J. Yellowlees

Book ID
113642072
Publisher
Elsevier Science
Year
2011
Tongue
English
Weight
697 KB
Volume
374
Category
Article
ISSN
0020-1693

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In the crystal structure of the title cocrystal, 2C 12 H 6 N 2 O 2 Á-C 2 H 6 N 4 O 2 , the diaminoglyoxime molecules are located on inversion centres, while the 1,10-phenanthroline-5,6-dione molecules are located in general positions. Both molecules are connected through intermolecular N-HÁ Á ÁO hyd

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## Abstract In order to monitor the progression of the synthesis and the separation of novel mixed‐ligand iron complexes containing 1,10‐phenanthroline, 1,10‐phenanthroline‐5,6‐dione, and NCS^−^ as ligands all products were mass analyzed by electrospray ionization ion trap MS/MS. The spectra of met