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Eigenschaften und Reaktionen von 1,1-Dimethoxy-2,6-diphenyl-λ5-phosphorin-4-carbaldehyd

✍ Scribed by Dimroth, Karl ;Pohl, Hans-Henning ;Wichmann, Karl-Heinz

Publisher
Wiley (John Wiley & Sons)
Year
1979
Tongue
English
Weight
975 KB
Volume
112
Category
Article
ISSN
0009-2940

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1,1-Dimethoxy-2,6-diphenyl-λ5-phosphorin
1,1-Dimethoxy-2,6-diphenyl-λ5-phosphorin-4-carbaldehyde and -4-carbonitrile
✍ Dr. Hans Henning Pohl; Prof. Karl Dimroth 📂 Article 📅 1975 🏛 John Wiley and Sons 🌐 English ⚖ 124 KB 👁 1 views

A well stirred solution of 3-methyllumiflavin~"1 (1.50g, 5.5 mmol) and N,N-dimethylpropargylamine (4.6 g, 55.0 mmol) in 0.1 M phosphate buffer (600 ml, pH 7.7) was illuminated under argon for 30 hours with a 170 W mercury high-piessure lamp (HERAEUS, Hanau; pyrex cooling jacket). The brown precipita