1,1-Dimethoxy-2,6-diphenyl-λ5-phosphorin
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Dr. Hans Henning Pohl; Prof. Karl Dimroth
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Article
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1975
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John Wiley and Sons
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English
⚖ 124 KB
A well stirred solution of 3-methyllumiflavin~"1 (1.50g, 5.5 mmol) and N,N-dimethylpropargylamine (4.6 g, 55.0 mmol) in 0.1 M phosphate buffer (600 ml, pH 7.7) was illuminated under argon for 30 hours with a 170 W mercury high-piessure lamp (HERAEUS, Hanau; pyrex cooling jacket). The brown precipita