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Synthese, Konstitution und Röntgenstrukturanalyse von 4,4-Bis(1,1-dimethoxy-2,6-diphenyl-λ5-phosphorin-4-ylmethyl)-1-methoxy-1-oxo-2,6-diphenyl-1,4-dihydro-λ5-phosphorin

✍ Scribed by Debaerdemaeker, Tony ;Pohl, Hans Henning ;Dimroth, Karl

Publisher
Wiley (John Wiley & Sons)
Year
1977
Tongue
English
Weight
387 KB
Volume
110
Category
Article
ISSN
0009-2940

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✦ Synopsis

Werte aus dem in den Benzolringen perdeuterierten 9.

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1,1-Dimethoxy-2,6-diphenyl-λ5-phosphorin
1,1-Dimethoxy-2,6-diphenyl-λ5-phosphorin-4-carbaldehyde and -4-carbonitrile
✍ Dr. Hans Henning Pohl; Prof. Karl Dimroth 📂 Article 📅 1975 🏛 John Wiley and Sons 🌐 English ⚖ 124 KB 👁 1 views

A well stirred solution of 3-methyllumiflavin~"1 (1.50g, 5.5 mmol) and N,N-dimethylpropargylamine (4.6 g, 55.0 mmol) in 0.1 M phosphate buffer (600 ml, pH 7.7) was illuminated under argon for 30 hours with a 170 W mercury high-piessure lamp (HERAEUS, Hanau; pyrex cooling jacket). The brown precipita