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EFFICIENT RESOLUTION OF (±)-1-(9-ANTHRYL)ETHYLAMINE

✍ Scribed by Roje, Marin; Hameršak, Zdenko; Šunjić, Vitomir

Book ID
123614775
Publisher
Taylor and Francis Group
Year
2002
Tongue
English
Weight
156 KB
Volume
32
Category
Article
ISSN
0039-7911

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📜 SIMILAR VOLUMES

Chemoenzymatic synthesis and properties
Chemoenzymatic synthesis and properties of Schiff bases containing (R)-1-(9-anthryl)ethylamine
✍ Marin Roje; Vitomir Šunjić 📂 Article 📅 2002 🏛 John Wiley and Sons 🌐 English ⚖ 113 KB

## Abstract Racemic 1‐(9‐anthryl)ethylamine (**10**), obtained in 70% overall yield from commercial 9‐cyanoanthracene, was kinetically resolved by the __Candida antarctica A__ lipase‐catalyzed acetylation with isopropyl acetate as acyl donor, affording (__R__)‐(+)‐**10** with 95.8% enantiomeric exc

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Enantioselective reduction of prochiral 9-anthryl ketones to the corresponding chiral alcohols proceeds with high enantiomeric excess. The chiral alcohol 1-(9-anthryl)-2-bromo-ethanol can be converted to the corresponding chiral oxirane. (~