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Efficient One-Pot Synthesis of Secondary Cyclic Phosphanes with Easy Regeneration of the Phosphorus-Donor Reagent Used.

✍ Scribed by Graziano Baccolini; Carla Boga; Matteo Galeotti

Publisher
John Wiley and Sons
Year
2004
Weight
71 KB
Volume
35
Category
Article
ISSN
0931-7597

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πŸ“œ SIMILAR VOLUMES

General and Efficient One-Pot Synthesis
General and Efficient One-Pot Synthesis of Tertiary Phosphane–Borane Complexes Containing Different Alkyl Groups and In Situ Facile Recycling of the Phosphorus Donor Reagent
✍ Graziano Baccolini; Carla Boga; Marzia Mazzacurati πŸ“‚ Article πŸ“… 2007 πŸ› John Wiley and Sons 🌐 English βš– 135 KB

## Abstract Tertiary symmetric and asymmetric phosphane–borane complexes containing different alkyl groups, including bulky groups, can be obtained by the addition of different Grignard reagents to benzothiadiphosphole **1** followed by direct complexation with BH~3~**Β·**THF. Treatment of the resul