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Efficient Lipase-Catalyzed Enantioselective Desymmetrization of Prochiral 2,2-Disubstituted 1,3-Propanediols and Meso 1,2-Diols Using 1-Ethoxyvinyl 2-Furoate

✍ Scribed by Akai, Shuji; Naka, Tadaatsu; Fujita, Tetsuya; Takebe, Yasushi; Tsujino, Toshiaki; Kita, Yasuyuki

Book ID
126938965
Publisher
American Chemical Society
Year
2002
Tongue
English
Weight
147 KB
Volume
67
Category
Article
ISSN
0022-3263

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ChemInform Abstract: Efficient Lipase-Ca
ChemInform Abstract: Efficient Lipase-Catalyzed Enantioselective Desymmetrization of Prochiral 2,2-Disubstituted 1,3-Propanediols and meso 1,2-Diols Using 1-Ethoxyvinyl 2-Furoate.
✍ Shuji Akai; Tadaatsu Naka; Tetsuya Fujita; Yasushi Takebe; Toshiaki Tsujino; Yas πŸ“‚ Article πŸ“… 2010 πŸ› John Wiley and Sons βš– 38 KB πŸ‘ 1 views

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Enzyme-catalyzed asymmetrization of 2,2-
Enzyme-catalyzed asymmetrization of 2,2-disubstituted 1,3-propanediols using 1-ethoxyvinyl esters
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The lipase-eatalyzed asymmetrization of the prochiral 2,2-disubstituted 1,3-propanediois 1, 6, and 9 was studied using various types of l-ethoxyvinyl esters 2. Among them, the use of the benzoate 2f provided good chemical and optical yields of the products 3, 7, and 10 bearing chiral quaternary carb

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Enzyme-Catalyzed Asymmetrization of 2,2-Disubstituted 1,3-Propanediols Using 1-Ethoxyvinyl Esters. -The lipase-mediated asymmetrization of prochiral diols using various 1-ethoxyvinyl esters (I) is studied. The benzoate ester (Ia) provides good to excellent chemical yields and the highest enantiosel