The vanillin residue makes dihedral angles of 4.84 (18) and 11.96 (7) with the planes of the butyl group and the terminal benzene ring, respectively. Intermolecular N-HÁ Á ÁO and C-HÁ Á ÁO hydrogen bonds help to consolidate the crystal packing.
(E)-N′-(3-Ethoxy-4-methoxybenzylidene)benzohydrazide
✍ Scribed by Zhen, Xiao-Li ;Han, Jian-Rong
- Publisher
- International Union of Crystallography
- Year
- 2005
- Tongue
- English
- Weight
- 152 KB
- Volume
- 61
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
In the title compound, C 17 H 18 N 2 O 3 , the isovanillin group makes a dihedral angle of 9.63 (11) with the plane of the terminal phenyl ring. Intermolecular N-HÁ Á ÁO hydrogen bonds help to consolidate the crystal packing.
📜 SIMILAR VOLUMES
In the title compound, C 16 H 16 N 2 O 4 Á0.5CH 3 CH 2 OH, the Schiff base is approximately planar. An intramolecular N-HÁ Á ÁO hydrogen bond stabilizes the molecular structure. The molecules are linked by O-HÁ Á ÁO hydrogen bonds to form a chain along the b axis.
An anhydrous ethanol solution of 4-benzyloxy-3-methoxybenzaldehyde (2.42 g, 10 mmol) was added to an anhydrous ethanol