N′-[(E)-4-(2-Hydroxyethoxy)-3-methoxybenzylidene]benzohydrazide monohydrate
✍ Scribed by Diao, Chun-Hua ;Yu, Ming ;Chen, Xin ;Jing, Zuo-Liang ;Deng, Qi-Liang
- Publisher
- International Union of Crystallography
- Year
- 2005
- Tongue
- English
- Weight
- 339 KB
- Volume
- 61
- Category
- Article
- ISSN
- 1600-5368
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📜 SIMILAR VOLUMES
An anhydrous ethanol solution of 4-benzyloxy-3-methoxybenzaldehyde (2.42 g, 10 mmol) was added to an anhydrous ethanol
The vanillin residue makes dihedral angles of 4.84 (18) and 11.96 (7) with the planes of the butyl group and the terminal benzene ring, respectively. Intermolecular N-HÁ Á ÁO and C-HÁ Á ÁO hydrogen bonds help to consolidate the crystal packing.
In the title compound, C 17 H 18 N 2 O 3 , the isovanillin group makes a dihedral angle of 9.63 (11) with the plane of the terminal phenyl ring. Intermolecular N-HÁ Á ÁO hydrogen bonds help to consolidate the crystal packing.
In the title compound, C 15 H 13 ClN 2 O 3 ÁH 2 O, the molecule adopts a trans configuration with respect to the C N double bond. The dihedral angle between the two rings is 15.03 (3) . The structure is stabilized by intramolecular O-HÁ Á ÁN and intermolecular N-HÁ Á ÁO and O-HÁ Á ÁO hydrogen bonds,