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(E)-1-(5-Bromo-3-meth­oxy-2-propoxybenzyl­idene)-2-(2,4-dinitro­phen­yl)hydrazine N,N-dimethyl­formamide solvate

✍ Scribed by Shi, Jun

Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
196 KB
Volume
62
Category
Article
ISSN
1600-5368

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✦ Synopsis

Single-crystal X-ray study T = 294 K Mean (C-C) = 0.005 A Disorder in main residue R factor = 0.041 wR factor = 0.106 Data-to-parameter ratio = 12.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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In the title compound, C~16~H~15~BrN~4~O~6~·C~3~H~7~NO, the substituted vanillin group makes a dihedral angle of 7.58 (10)° with the nitrophenylhydrazine mean plane. A bifurcated intra/intermolecular N—H...(O,O) hydrogen bond and two C—H...O interactions help to establish the molecular conformation

(E)-1-[2-(2-Chloro­benz­yloxy)benzyl­ide
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✍ Shi, Jun 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 158 KB

Single-crystal X-ray study T = 294 K Mean (C-C) = 0.004 A Disorder in solvent or counterion R factor = 0.043 wR factor = 0.146 Data-to-parameter ratio = 11.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.