The molecule of the title compound, C 20 H 18 N 4 O 6 ÁC 3 H 3 N, is non-planar. The central benzene ring makes dihedral angles of 85.73 (10) and 2.70 (12) with the terminal phenyl ring and the nitrophenylhydrazine mean plane, respectively. An intramolecular N-HÁ Á ÁO hydrogen bond helps to establis
(E)-1-[2-(Benzyloxy)-3-methoxybenzylidene]-2-(2,4-dinitrophenyl)hydrazine dimethylformamide solvate
✍ Scribed by Shi, Jun
- Publisher
- International Union of Crystallography
- Year
- 2006
- Tongue
- English
- Weight
- 173 KB
- Volume
- 62
- Category
- Article
- ISSN
- 1600-5368
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📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 294 K Mean (C-C) = 0.004 A Disorder in solvent or counterion R factor = 0.043 wR factor = 0.146 Data-to-parameter ratio = 11.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
In the title compound, C~16~H~15~BrN~4~O~6~·C~3~H~7~NO, the substituted vanillin group makes a dihedral angle of 7.58 (10)° with the nitrophenylhydrazine mean plane. A bifurcated intra/intermolecular N—H...(O,O) hydrogen bond and two C—H...O interactions help to establish the molecular conformation