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dl-Aspartic acid

✍ Scribed by Wang, Guo-Ming ;Li, Zeng-Xin ;Duan, Chun-Sheng ;Li, Hui


Publisher
International Union of Crystallography
Year
2007
Tongue
English
Weight
751 KB
Volume
63
Category
Article
ISSN
1600-5368

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A synthesis of the title compound from /13Clparaformaldehyde and [15N)ammonium chloride V f 8 ethyl 2-(1 ,3-/2-13Cldithianyl) acetate 3a is described. Ethyl/3-13C13-oxopropanoate derived in sl'tu from 3a was converted by a stepwise Strecker procedure to DL-[ 2-13C,15Nlaspartic acid 7a.

Solubilities ofL-aspartic,DL-aspartic,DL
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Solubilities of L-aspartic, DL-aspartic, DL-glutaric, p-hydroxybenzoic, o-anisic, p-anisic, and itaconic acids in water were determined in the temperature range 278 to 345 K. From these solubilities the apparent molar enthalpies of solution at T s 298.15 K were derived, and these . y1 . y1 Ε½ . Ε½ are

l-Aspartic acid nitrate–l-aspartic acid
✍ Sridhar, B. ;Srinivasan, N. ;Rajaram, R. K. πŸ“‚ Article πŸ“… 2002 πŸ› International Union of Crystallography 🌐 English βš– 400 KB

Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.007 A Ê R factor = 0.041 wR factor = 0.118 Data-to-parameter ratio = 7.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.