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Divergent Synthesis of Cytotoxic Styryl Lactones from d -Xylose. The First Total Synthesis of (+)-Crassalactone C

✍ Scribed by Popsavin, Velimir; Benedeković, Goran; Srećo, Bojana; Popsavin, Mirjana; Francuz, Jovana; Kojić, Vesna; Bogdanović, Gordana

Book ID
126864876
Publisher
American Chemical Society
Year
2007
Tongue
English
Weight
84 KB
Volume
9
Category
Article
ISSN
1523-7060

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Divergent synthesis of cytotoxic styryl
Divergent synthesis of cytotoxic styryl lactones isolated from Polyalthia crassa. The first total synthesis of crassalactone B
✍ Velimir Popsavin; Goran Benedeković; Mirjana Popsavin; Vesna Kojić; Gordana Bogd 📂 Article 📅 2010 🏛 Elsevier Science 🌐 French ⚖ 297 KB

The first total synthesis of (+)-crassalactone B (2) and a new syntheses of (+)-crassalactone C (3) has been achieved starting from D-glucose. The natural products 2 and 3 can be selectively accessed by changing the conditions for TBDPS cleavage in the final intermediate 16. The synthesized natural