Single-crystal X-ray study T = 150 K Mean '(C±C) = 0.006 A Ê Disorder in main residue R factor = 0.053 wR factor = 0.154 Data-to-parameter ratio = 7.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Disordered 2,2′,3,3′,4,6,6′-hepta-O-pivaloyl-α,α′-trehalose
✍ Scribed by Baddeley, Thomas C. ;Clow, Simon M. ;Cox, Philip J. ;Davidson, Iain G. ;Murdoch, Alison M. ;Wardell, James L.
- Publisher
- International Union of Crystallography
- Year
- 2003
- Tongue
- English
- Weight
- 314 KB
- Volume
- 59
- Category
- Article
- ISSN
- 1600-5368
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## Abstract Die Glycosylierung von Benzylalkohol und Cholesterin gelingt mit 2,3,4,6‐Tetra‐__O__‐pivaloyl‐α‐D‐glucopyranosylbromid **(2)** in Gegenwart von Silbersalzen in hoher Ausbeute. Die bei Koenigs‐Knorr‐Synthesen mit 2,3,4,6‐Tetra‐__O__‐acetyl‐α‐D‐glucopyranosylbromid **(5)** störende Orthoe
11. and Raman spectra of solid a,a-trehalose and a,a-trehalose-2,3,4.6,6-6,, in the C-H and C-D stretching regions are recorded. The experimental data are reproduced satisfactorily by normal co-ordinate and i.r. absorption intensity calculations which take into account the specific interactions of e