✦ LIBER ✦

Direct preparation of 14C-labeled 5-allyl- and 5-propyl-2′-deoxyuridine from [2- 14C]2′-deoxyuridine

✍ Scribed by Jerry L. Ruth; Steven K. White; Donald E. Bergstrom

Publisher: John Wiley and Sons
Year: 1982
Tongue: French
Weight: 246 KB
Volume: 19
Category: Article
ISSN: 0022-2135
DOI: 10.1002/jlcr.2580190706

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✦ Synopsis

Abstract

[2‐^14^C]5‐Allyl‐2′‐deoxyuridine was synthesized directly from [2‐^14^C]2′‐deoxyuridine using mercury, palladium, and 3‐chloropropene. [2‐^14^C]5‐Propyl‐2′‐deoxyuridine was obtained by hydrogenation of the [^14^C]5‐allyl‐2′‐deoxy‐uridine. Advantages of the synthetic method and its application to the preparation of other radiolabeled 5‐alkyl/alkeny1‐2′‐deoxyuridines are discussed.

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