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Direct ortho -Arylation of ortho -Substituted Benzoic Acids: Overriding Pd-Catalyzed Protodecarboxylation

✍ Scribed by Arroniz, Carlos; Ironmonger, Alan; Rassias, Gerry; Larrosa, Igor

Book ID: 118741575
Publisher: American Chemical Society
Year: 2013
Tongue: English
Weight: 399 KB
Volume: 15
Category: Article
ISSN: 1523-7060
DOI: 10.1021/ol400065j

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## Abstract Direct synthesis of γ‐substituted phthalids from related __ortho__‐aryl benzoic acids with 48–85% yield are covered. The direct oxidation in the presence of peroxydisulphate‐copper (II) chloride in aqueous medium was applied. The reaction is highly regioselective and leads exclusively t