Dipyridine(2,3,12,13-tetrabromo-5,10,15,20-tetraphenylporphyrin)iron(II) pyridine solvate
✍ Scribed by Scheidt, W. Robert ;Noll, Bruce C.
- Publisher
- International Union of Crystallography
- Year
- 2006
- Tongue
- English
- Weight
- 330 KB
- Volume
- 62
- Category
- Article
- ISSN
- 1600-5368
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📜 SIMILAR VOLUMES
Single-crystal synchrotron study T = 150 K Mean '(C±C) = 0.003 A Ê R factor = 0.052 wR factor = 0.129 Data-to-parameter ratio = 23.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Single-crystal synchrotron study T = 160 K Mean '(C±C) = 0.004 A Ê Disorder in main residue R factor = 0.054 wR factor = 0.135 Data-to-parameter ratio = 16.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
The structure of the title compound, [Zn(C 92 H 60 N 4 )-(C 2 H 3 N)]ÁC 2 H 3 N, shows relatively small saddle-type distortion with ruf¯ing, compared to other dodecaphenylporphyrin complexes.
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.006 A Ê Disorder in solvent or counterion R factor = 0.047 wR factor = 0.159 Data-to-parameter ratio = 15.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.