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[μ-10,21-Di-tert-butyl-4(S),5(S),15(S),16(S)-tetra­phenyl-3,6,14,17-tetra­aza­tri­cyclo­[17.3.1.18,12]­tetracosa-1(23),2,6,8,10,12(24),13,17,19,21-decaene-23,24-diolato](μ-ethyl­ene glycol)­dinickel(II) diperchlorate dihydrate

✍ Scribed by Wu, Jin-Cai ;Li, Yi-Zhi ;Tang, Ning ;Tan, Min-Yu

Publisher
International Union of Crystallography
Year
2003
Tongue
English
Weight
339 KB
Volume
59
Category
Article
ISSN
1600-5368

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✦ Synopsis

Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.006 A Ê Disorder in solvent or counterion R factor = 0.047 wR factor = 0.159 Data-to-parameter ratio = 15.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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The title complex, [Cu~2~(C~20~H~16~F~2~N~4~O~2~)(CH~4~O)~2~](ClO~4~)~2~, was synthesized by cyclo-condensation between ethylenediamine and 2,6-diformyl-4-fluorophenol in the presence of Cu^II^ ions. This dinuclear copper complex is centrosymmetric. Both Cu atoms are in a distorted tetrahedral geome