Synthesis and Crystal Structure of a New
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Sabine Herzog; Christian Näther; Peter Dürichen; Wolfgang Bensch
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Article
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1998
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John Wiley and Sons
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German
⚖ 93 KB
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Needle-shaped, moisture sensitive, yellow crystals of Na 3 TaS 4 were obtained by the reaction of Na 2 S 3 , Ta, and S at 450 °C. The structure was determined by single crystal X-ray diffraction and refined to R1 and wR2 values of 0.0172 and 0.0381, respectively. Na 3 TaS 4 crystallizes with 32 form