Dimethylbis(2-methylquinolin-8-olato-κ 2N , O )tin(IV)
✍ Scribed by Najafi, Ezzatollah; Amini, Mostafa M.; Ng, Seik Weng
- Book ID
- 125423095
- Publisher
- International Union of Crystallography
- Year
- 2012
- Tongue
- English
- Weight
- 271 KB
- Volume
- 68
- Category
- Article
- ISSN
- 1600-5368
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📜 SIMILAR VOLUMES
The five-coordinate geometry of the Al atom in the title compound, [Al(C 10 H 8 NO) 2 (C 16 H 11 O)], is trigonal-bipyramidal, in which the O-donor atoms of the naphtholate and the two quinolinolate ligands are in the trigonal equatorial plane and the N atoms in the axial positions.
Single-crystal X-ray study T = 299 K Mean (C-C) = 0.012 A R factor = 0.062 wR factor = 0.154 Data-to-parameter ratio = 12.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
A methanol solution (5 ml) of 8-hydroxyquinoline (0.075 g, 0.5 mmol) was mixed with an aqueous solution (5 ml) of AgNO 3