Dibromo(1,4-dioxan)tin(II): the crystal structure
β Scribed by Andrews, R. H. ;Donaldson, J. D. ;Hough, E. ;Nicholson, D. G.
- Book ID
- 114523901
- Publisher
- International Union of Crystallography
- Year
- 1977
- Weight
- 200 KB
- Volume
- 33
- Category
- Article
- ISSN
- 0567-7408
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## Abstract __trans__β2,3βDibromoβ1,4βdioxan crystallizes in the orthorhombic system, space group P2~1~2~1~2~1~, Z = 4, with cell dimensions: a = 5.68^5^, b = 7.59, c = 15.82 Γ at β100Β°. The structure was refined in two centrosymmetric projections by means of reflexion data obtained at β100Β° using
The title compound (C 10 H 10 O 2 Br 2 ) crystallizes in the orthorhombic space group P2 1 2 1 2 1 with a = 5.0319(2)Γ , b = 13.5282(5)Γ , c = 15.6289(6)Γ , V = 1063.90(1)Γ 3 , Z = 4, D x = 2.01 g/cm 3 at T = 293(2)K. The structure was solved by direct methods and refined by full-matrix least-squares p