𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Di-μ-chloro-bis­[(2,2′:6,2′′-ter­pyridine-κ3N)copper(II)] diperchlorate: the triclinic polymorph

✍ Scribed by Gasser, Gilles ;Labat, Gaël ;Stoeckli-Evans, Helen

Publisher
International Union of Crystallography
Year
2004
Tongue
English
Weight
367 KB
Volume
60
Category
Article
ISSN
1600-5368

No coin nor oath required. For personal study only.

✦ Synopsis

Single-crystal X-ray study T = 153 K Mean '(C±C) = 0.015 A Ê R factor = 0.068 wR factor = 0.185 Data-to-parameter ratio = 12.9

For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

📜 SIMILAR VOLUMES

(2,2′-Bi­pyridine-κ2N,N′)­di­chloro­copp
(2,2′-Bi­pyridine-κ2N,N′)­di­chloro­copper(II)
✍ Wang, Yan-Qin ;Bi, Wen-Hua ;Li, Xing ;Cao, Rong 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 357 KB

The title compound, [CuCl 2 (C 10 H 8 N 2 )], has twofold symmetry and the coordination geometry around the Cu II atom is distorted square-planar. There are weak intermolecular CuÁ Á ÁCl interactions, forming a chain structure in the crystal.

Di­iodo(4′-phenyl-2,2′:6′,2′′-ter­pyridi
Di­iodo(4′-phenyl-2,2′:6′,2′′-ter­pyridine-κ3N)copper(II)
✍ Hou, Lei ;Li, Dan ;Wu, Tao ;Yin, Ye-Gao ;Ng, Seik Weng 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 171 KB

Single-crystal X-ray study T = 295 K Mean '(C±C) = 0.009 A Ê R factor = 0.040 wR factor = 0.111 Data-to-parameter ratio = 14.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

{μ-9,10-Bis­[(n-propyl­amino)­methyl]­an
{μ-9,10-Bis­[(n-propyl­amino)­methyl]­anthracene-κ2N:N′}bis{bis­[6-chloro-2-(di­phenyl­phosphino)­pyridine-κP]copper(I)} diperchlorate
✍ Xu, Feng-Bo ;Xu, Hu ;Leng, Xue-Bing ;Song, Hai-Bin ;Li, Qing-Shan ;Zou, Ru-Yi ;Z 📂 Article 📅 2003 🏛 International Union of Crystallography 🌐 English ⚖ 304 KB

The title compound, [Cu 2 (C 15 H 13 ClP) 4 (C 30 H 28 N 2 )](ClO 4 ) 2 , was synthesized by the reaction of 9,10-bis[(n-propylamino)methyl]anthracene and 6-chloro-2-(diphenylphosphino)pyridine with [Cu(CH 3 CN) 4 ]ClO 4 . The Cu atoms adopt a trigonal±planar geometry and the cation is centrosymmetr