The analytical performance of a platinum preconcentration method using a 0.01 M HNO, carrier solution and an alumina microcolumn is discussed. On-line preconcentration is followed by flame atomic absorption spectrometry (FAAS), and off-line preconcentration by graphite furnace atomic absorption spec
Determination of trace amounts of lead by chelating ion exchange and on-line preconcentration in flow-injection atomic absorption spectrometry
β Scribed by Rajesh Purohit; Surekha Devi
- Publisher
- Elsevier Science
- Year
- 1992
- Tongue
- English
- Weight
- 552 KB
- Volume
- 259
- Category
- Article
- ISSN
- 0003-2670
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β¦ Synopsis
Resins synthesized from qumohn-b-01 and resorcmol or hydroqmnone, with furfuraldehyde, formaldehyde or benzaldehyde as cross-hnkmg agent, were used for the preconcentrafion of nanogram amounts of lead The rate of exchange and activation energy of lead exchange were calculated Column separations of lead-copper and lead-zmc did not show any cross-contarnmation A contmuous-flow manifold usmg resin rmcrocolumns was developed for the preconcentration and determmation of lead
π SIMILAR VOLUMES
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A flow injection on-line coprecipitation preconcentration system with diethyldithiocarbamate (DDTC) chelate of copper used as the coprecipitate carrier was coupled with flame atomic absorption spectrometry (FAAS) for the determination of trace silver. Silver was on-line coprecipitated with DDTC-Cu(I
Methods are described for the determination of ultratrace amounts of copper and cadmium in seawater by graphite furnace atomic absorption spectrometry with flow-injection, microcolumn preconcentration. A new type of \(\mathrm{C}_{18}\) column loaded with sodium diethyldithiocarbamate (sodium-DDC) wa
A desolvation device was connected to a microcolumn (40 mm X 3.0 mm i.d.) in which 8-hydroxyquinoline-5sulphonic acid was immobilized on the substrate of active carbon-silica gel. The analyte and 1.0 M sodium acetate-acetic acid buffer solution (pH 5.6) were mined and pumped through the microcolumn.