Determination of surface hydroxyl concentration on glass and fused silica capillary columns
โ Scribed by B. W. Wright; P. A. Peaden; M. L. Lee; G. M. Booth
- Book ID
- 112723708
- Publisher
- Springer
- Year
- 1982
- Tongue
- English
- Weight
- 274 KB
- Volume
- 15
- Category
- Article
- ISSN
- 0009-5893
No coin nor oath required. For personal study only.
๐ SIMILAR VOLUMES
The life expectancy and resistance to flow, pressure shocks, solvent gradients, and bending of packed fused silica capillary columns (Micro-LC) are discussed. ## 2 Instrumentation Chromatographic measurements were carried out on a Varian 5020 (Varian Associates, Walnut Creek, CA, USA) and on a Per
## Chromatography bony1 functional groups at bonded silanol sites on the surface. It is further shown that simple test mixtures containing aldehydes or ketones can be used to probe the concentration of water and bonded silanols on the surface and thus to evaluate capillary manufacturing processes
A study was carried out on the effects of acid leaching of capillary column wall materials. Leaching experiments with glass and fused silica were performed under static and dynamic conditions; moreover, the influence of the temperature was investigated. The amount of water released during different
A 30 m, 0.25 mm ID, fused silica capillary column at temperatures from -60 to -1 OOOC has been shown to be a quantitative trap for organic compounds with volatilities ranging from that of 1 ,I -dichloroethene to that of chlorobenzene.Thistypeof "whole column cryotrapping" provided sharp peaks (peak