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Determination of methylguanidine in plasma and urine by high-performance liquid chromatography with fluorescence detection following postcolumn derivatization

โœ Scribed by Venkata K. Boppana; Gerald R. Rhodes; David P. Brooks

Publisher
Elsevier Science
Year
1990
Tongue
English
Weight
565 KB
Volume
184
Category
Article
ISSN
0003-2697

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## Abstract A simple, specific and sensitive HPLC method has been developed for the determination of metoprolol in human plasma and urine. Separation of metoprolol and atenolol (internal standard) was achieved on an Ace C~18~ column (5โ€‰ฮผm, 250โ€‰mmร—4.6โ€‰mm id) using fluorescence detection with ฮป~ex~=2