Two standard titrimetric procedures for determination of free fatty acids in vegetable oils and in oils extracted from oilseeds were examined using rapeseed oil, illipe nuts and fat, and groundnuts and groundnut oil as test materials. Both procedures involve dissolution of the fat in an organic solv
Determination of free fatty acids and diacylglycerols in native vegetable oils
✍ Scribed by Brühl, Ludger
- Publisher
- John Wiley and Sons
- Year
- 1997
- Weight
- 503 KB
- Volume
- 99
- Category
- Article
- ISSN
- 0931-5985
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✦ Synopsis
The analysis of free fatty acids (FFA) and diacylglycerols (DG) by GLC may be used to detect the deacidification of oils. Free fatty acids are removed from the oil during neutralization or physical refining, while the corresponding DG remain in the oil. This will change the ratio of FFA to DG. For analysis, oils with tricaprin as internal standard are silylated and injected on-column onto a short high-temperature capillary column. Extracted oils showed higher amounts of FFA and DG than pressed oils from the same batch of seeds. There are only minor changes in the ratio of FFA to DG according to the yield of pressing or due to washing the oil.
Bestimmung von freien Fettslluren und Diacylglycerolen in rohen Pflanrendlen.
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