𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Determination of Enantiomeric Excess of Leucine by13C CP-MAS Solid-State NMR

✍ Scribed by E. J. Tadeusiak; W. Ciesielski; S. Olejniczak


Book ID
106220509
Publisher
Springer Vienna
Year
2008
Tongue
English
Weight
278 KB
Volume
35
Category
Article
ISSN
0937-9347

No coin nor oath required. For personal study only.


πŸ“œ SIMILAR VOLUMES


Detecting 13C in solid pitches by CP/MAS
✍ Pierre Ollivier; B.C. Gerstein πŸ“‚ Article πŸ“… 1984 πŸ› Elsevier Science 🌐 English βš– 315 KB

## A~~act~ompa~~n of "C NMR spectra in solid pitches taken under conditions of: cross polarization with strong proton decoupling, but no sample rotation (CP), and cross polarization with strong proton decoupling and magic angle sample spinning (CP/MAS) indicate that there is a considerable loss of

Determination of enantiomeric excess by
✍ V. N. Gogte; R. K. Nanda; A. A. Natu; V. S. Pandit; M. K. Sastry πŸ“‚ Article πŸ“… 1984 πŸ› John Wiley and Sons 🌐 English βš– 283 KB

Oxazolidine derivatives of p-amino alcohols such as ephedrine have been resolved by -C NMR spedroscopy using Eu(hfc), as a chiral shift reagent. The method is quantitative in the determination of enantiomeric excess, and is advantageous where 'H NMR is of limited use owing, for example, to signitica

Solid-State 13C CP/MAS NMR Investigation
✍ Todd M. Alam; Roger A. Assink πŸ“‚ Article πŸ“… 1997 πŸ› John Wiley and Sons 🌐 English βš– 312 KB πŸ‘ 2 views

Solid-state 13C CP/MAS NMR spectra are reported for di †erent EDTA-metal complexes. The e †ect of metal binding on the isotropic 13C chemical shift and principal elements of the carboxyl 13C chemical shift anisotropy (CSA) tensor are discussed.

High-resolution solid-state 13C CP/MAS N
✍ M. Bardet; A. Rousseau; M. Vincendon πŸ“‚ Article πŸ“… 1993 πŸ› John Wiley and Sons 🌐 English βš– 554 KB

## Abstract Scleroglucan is a branched poiysaccharide, soluble in water. Solid‐state and solution ^13^C NMR were used to follow the fixation of water molecules on anhydrous scleroglucan and the evolution of the scleroglucanβ€”water complex from the solid state to the gel and solution state. Determina