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Determination of carbonyl group position in triamantanone by13C-NMR Spectroscopy

✍ Scribed by Z. Kafka; L. Vodička; M. Hájek

Book ID
112368742
Publisher
Springer
Year
1984
Tongue
English
Weight
189 KB
Volume
318
Category
Article
ISSN
1618-2650

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Determination of enantiomeric excess by
Determination of enantiomeric excess by 13C NMR spectroscopy
✍ V. N. Gogte; R. K. Nanda; A. A. Natu; V. S. Pandit; M. K. Sastry 📂 Article 📅 1984 🏛 John Wiley and Sons 🌐 English ⚖ 283 KB

Oxazolidine derivatives of p-amino alcohols such as ephedrine have been resolved by -C NMR spedroscopy using Eu(hfc), as a chiral shift reagent. The method is quantitative in the determination of enantiomeric excess, and is advantageous where 'H NMR is of limited use owing, for example, to signitica