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Determination of Absolute Configuration of Acyclic 1,2-Diols with Mo2(OAc)4. 1. Snatzke's Method Revisited

✍ Scribed by Di Bari, Lorenzo; Pescitelli, Gennaro; Pratelli, Carmela; Pini, Dario; Salvadori, Piero

Book ID
111867753
Publisher
American Chemical Society
Year
2001
Tongue
English
Weight
184 KB
Volume
66
Category
Article
ISSN
0022-3263

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The in situ complexes of dimolybdenum tetraacetate [Mo 2 (OAc) 4 ] with vicinal diols give CD spectra suitable for determination of their absolute configuration. Positive (negative) torsional angle in the O-C-C-O moiety leads to a positive (negative) Cotton effect at around 300 nm. The extension of