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Application of [Mo2(OAc)4] for determination of absolute configuration of pyranoid and furanoid vic-diols by circular dichroism

✍ Scribed by Jadwiga Frelek; Zbigniew Pakulski; Aleksander Zamojski

Publisher
Elsevier Science
Year
1996
Tongue
English
Weight
443 KB
Volume
7
Category
Article
ISSN
0957-4166

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The in situ complexes of dimolybdenum tetraacetate [Mo 2 (OAc) 4 ] with vicinal diols give CD spectra suitable for determination of their absolute configuration. Positive (negative) torsional angle in the O-C-C-O moiety leads to a positive (negative) Cotton effect at around 300 nm. The extension of