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Determination of 4-(4-chlorophenyl)-4-hydroxypiperidine, a metabolite of haloperidol, by gas chromatography with electron-capture detection

✍ Scribed by Jian Fang; Glen B. Baker; Ronald T. Coutts

Publisher
Elsevier Science
Year
1996
Weight
478 KB
Volume
682
Category
Article
ISSN
0378-4347

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## Abstract A sensitive GC‐ECD assay has been developed for the simultaneous determination of midazolam (I) and its α‐hydroxy metabolite (II) in plasma. The assay involves extraction of both compounds into ether at alkaline pH (pH 12), followed by silylation of the α‐hydroxy metabolite with N,O‐bis