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Detection and identification of the plant lignans lariciresinol, isolariciresinol and secoisolariciresinol in human urine

✍ Scribed by C. Bannwart; H. Adlercreutz; K. Wähälä; G. Brunow; T. Hase

Book ID: 115826355
Publisher: Elsevier Science
Year: 1989
Tongue: English
Weight: 632 KB
Volume: 180
Category: Article
ISSN: 0009-8981
DOI: 10.1016/0009-8981(89)90011-9

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The heptafluorobutyryl derivatives of some steroid standards were analyzed on a 25 m X 0.32 mm OV-1 fused silicacolumn. The effluent was split in the ratio : FID 5 : ECD 1 by using split arms of 20 cm X 0.32 mm ID and 20 X 0.25 mm ID respectively. Make-up gas was nitrogen with a flow-rate of 22 ml m