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Derivatives of potassium cyanodithioimidocarbonate. I. Synthesis of 1,4,6,9-tetrathiaspiro[4.4]nonane and related compounds

✍ Scribed by D'Amico, John J.; Campbell, Robert Henry

Book ID
127392365
Publisher
American Chemical Society
Year
1967
Tongue
English
Weight
590 KB
Volume
32
Category
Article
ISSN
0022-3263

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## Abstract 8,9‐Benzo‐2‐methylene‐1,4,6‐trioxaspiro[4,4]nonane (BMTN) was prepared by the reaction of phthalide with epichlorohydrin, followed by dehydrochlorination. BMTN was polymerized with di‐__t__‐butyl peroxide (DTBP) to give a solyble polymer with a high molecular weight and good thermal sta